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OptiMelt References                                            www.thinkSRS.com



OptiMelt References

Measurement and Theory
  1. Kenneth Nolon Carter and Kenneth N. Carter, Jr., "Meaningful Melting
     Points", J. Chem. Educ. 72 (1995) 647. Note: A very careful study of MP
     determinations and the proper way to observe and document results and
     observations.
  2. Martin Davidson, "Avoiding Errors in Melting Point Determinations",
     International Labmate, vol. 23, issue 4, July 1998.
  3. Gail Karet, "Make the Most of Melting Point Measurements", R&D
     Magazine, July 1999, p. 61
  4. Sharp, J. T., Gosney J. and Rowley A. G., "Practical Organic Chemistry, A
     Student Handbook of Techniques", 1999, Chapman & Hall, NY, USA.
  5. Donal Pavia, et. Al., "Introduction to Organic Laboratory Techniques: A
     Microscale Appproach", 1st edition, Saunders College Publishing,
     Philadelphia, USA, 1990.
  6. R. L. Shriner, R. C. Fuson and D. Y. Curtin, "Systematic Identification of
     Organic Compounds", 5th edition, 1966, Wiley International, NY, USA,
     Chapter 4, p. 28-34.
  9. W. J. Criddle, Gwynn P. Ellis, "Spectral and Chemical Characterization of
     Organic Compounds: A Laboratory Handbook", 3rd edition, 1990,Wiley,
     John and Sons.
  7. Harding, Ken E., "Melting Point Range and Phase Diagrams- Confusing
     Laboratory Textbook Descriptions", J. Chem. Educ. 76 (1999) 224.
  8. Brown, R. J. C.; Brown, R. F. C., "Melting Point and Molecular Symmetry",
     J. Chem. Educ. 77(2000) 724.
  10. George V. D. Tiers, "Melting Points are Uncorrected"-True or False?, J.
     Chem. Educ., 67 (1990) 258



             Stanford Research Systems, Inc.                 Phone: (408) 744-9040
OptiMelt References                                             www.thinkSRS.com


  11. George V. D. Tiers, "Calibration of capillary melting point apparatus to the
     International Temperature Scale of 1990 (ITS-90) by use of fluxed highly
     pure metals", Analytica Chimica Acta, 237 (1990) 241
  12. "OECD Guidelines for the Testing of Chemicals, Test No. 102: Melting
     Point/ Melting Range", OECD Organisation for Economic Co-operation
     and Development, January 2001, vol. 1, no. 1, pp. 1-8 (8 pages). Note:
     The OECD Guidelines for the Testing of Chemicals are a collection of
     about 100 of the most relevant internationally agreed testing methods
     used by government, industry and independent laboratories to identify and
     characterize potential hazards of new and existing chemical substances,
     chemical preparations and chemical mixtures. Adopted in 1981, the
     Guidelines have become the recognized reference tool for professionals
     working on the testing of chemicals and the assessment of their potential
     hazards. Purchase guidelines on-line at: http://www.sourceoecd.org/
  13. Randal A. Gauthier, "Time to Learn your RTDs", Sensors, May 2003, p.
     53. Note: Pt RTDs aare discussed in detail, along with some aging
     guidelines.


  MP Tables
  1. W. Utermark, "Melting Point Tables of Organic Compounds". 2nd revised
     and supplemented edition. Interscience: New York, 1963. Note: Provides
     data for over 7000 compounds, arranged by increasing melting point
     temperatures. While not used much today for research purposes, this
     work is still valuable as a teaching tool.
  2. David R. Lide, "The Handbook of Chemistry & Physics", CRC Press, 2003.
  3. Patricia Heckelman, Ann Smith (Editor), Maryadele J. Oneil (Editor), "
     Merck Index: An Encyclopedia of Chemicals, Drugs & Biologicals- 13th
     Edition ", Merck Publishing Group , Merck &Company Inc., 2001.




             Stanford Research Systems, Inc.                  Phone: (408) 744-9040
OptiMelt References                                                www.thinkSRS.com


  4. Amyand David Buckingham (Editor), Finlay J. MacDonald (Editor),
     "Dictionary of Organic Compounds", CRC Press, 1995.
  5. John A. Dean, Norbert Adolph Lange, "Lange's Handbook of Chemistry",
     The McGraw-Hill Companies, 1998.
  6. W. L. F. Armargo and D. D. Perrin, "Purification of Laboratory Chemicals",
     4th edition, Butterworth Heinemann, Woburn, MA, USA, 1998.
  7. R. L. Shriner, R. C. Fuson and D. Y. Curtin, "Systematic Identification of
     Organic Compounds", 5th edition, 1966, Wiley International, NY, USA,
     Chapter 4, p. 28-34.
  8. "Aldrich Handbook of Fine Chemicals and Laboratory Equipment", Sigma-
     Aldrich Fine Chemicals, P.O. Box 355, Milwaukee, WI 53201, USA, 2003-
     2004 (www.sigma-aldrich.com.)
  9. W. J. Criddle, Gwynn P. Ellis, "Spectral and Chemical Characterization of
     Organic Compounds: A Laboratory Handbook", 3rd edition, 1990,Wiley,
     John and Sons.
  10. Zvi Rappoport (Editor), "Handbook of Tables for Organic Compound
     Identification", CRC Press, 1966.
  11. Farmilo, C. G. and Levi, L.: Part IA:" Introduction to identification of
     narcotics by physical methods", Bulletin on Narcotics, Vol. V, No. 4. Note:
     Farmilo and Levi have written several articles on the identification of
     narcotics centered around melting point determinations.
  12. Beilstein Files, http://info.cas.org/ONLINE/DBSS/beilstein.html. Database
     provided by: MDL Information Systems GmbH, Theodor-Heuss-Allee 108,
     D-60486 Frankfurt, Germany, STNmail: HLPBEILK, Phone:(+49) 69/5050-
     4252, Fax:(+49) 69/5050-4245, E-mail: [email protected]. Note: this
     database includes over 8 million compounds but requires subscription and
     dedicated client software.




              Stanford Research Systems, Inc.                    Phone: (408) 744-9040
OptiMelt References                                            www.thinkSRS.com



  Quality Control

  GLP and GMP


  1. Ludwig Huber, "Validation and Qualification in Analytical Laboratories",
     Interpharm Press, Buffalo Grove, IL, USA, 1998.
  2. Ludwig Huber, "A primer - Good Laboratory Practice and Current Good
     Manufacturing Practice", Publication # 5968-6193E, Agilent Technologies,
     Germany, March 2000.
  3. Ludwig Huber, "Validation of Computerized Analytical and Networked
     Systems", CRC Press, 2002.
  4. Michael Anisfeld, "International Drug GMPs", Interpharm Press, Buffalo
     Grove, IL, USA, August 1993.
  5. Michael H. Anisfeld (Editor), " International GLPs", CRC Press, 1993.


Pharmacopoeias


  1. "International Pharmacopoeia: Tests, Methods, and General
     Requirements: Quality Specifications for Pharmaceutical Substances,
     Excipients, and Dosage Forms", 3rd edition, volume 5, published by
     WHO Staff, www.who.int (order at www.bookorders.who.int).
  2. "United States Pharmacopoeia", USP 27



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