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5991-4865EN Evaluation of Bearing Materials Using Nano-Scale Wear Testing - Application Note c20140808 [6]


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Keysight Technologies
Evaluation of Bearing Materials Using
Nano-Scale Wear Testing




                              Application Note
Introduction

     The most common materials for bearing fabrication are metals, such as low-carbon steel, stainless
     steel, chrome steel and high-speed steel. Polymeric materials are alternative candidates due to
     their self-lubrication ability, high impact durability, high corrosion resistance, low specific gravity,
     and high melting temperature. Polymers have therefore received widespread attention as new
     tribological materials for dry, aqueous and corrosive conditions. Among these polymeric materials,
     polytetrafluoroethylene (PTFE), polyether ether ketone (PEEK) and also their composites are often used
     in tribological applications.

     In fans used for cooling of computers and other electronics, it has been found that one of the main
     contributors to failure is degradation of the miniature ball bearings [1], with deterioration of the
     lubricant as the primary failure mechanism in these applications. Due to the criticality of ball bearings,
     diagnosis and prognosis of these failures have been of interest to the industry. There are several
     techniques to detect faults in ball bearings. In 2011 Oh, et al, found a correlation between acoustic
     emission (AE) features and bearing degradation in computer cooling fans [2]. More recently, in 2013
     Kumar, et al [3] determined the failure mechanisms of polymeric bearings using the analysis of vibration,
     speed and acoustic emission data, together with characterization of the worn bearing surfaces and
     measurements of friction.

     The bearing materials tested in this work were previously evaluated [3] at a rotational speed of 4800rpm
     in a test fixture which supports a load of approximately 1.4N. Acoustic emissions from these bearings
     during the initial stages of the operation of the bearings were monitored to compare the performance
     of these materials. These prior results are shown in Figure 1. Throughout most of the AE test, and
     especially near the end, the steel bearings exhibited the fewest AE events, followed by the PEEK and the
     PTFE bearings. Thus, from the AE test, we would rank the materials in order of performance (from best
     to worst) as: bearing steel, PEEK, PTFE.

     However, AE testing requires a long time. Thus, the aim of the present work is to establish a rapid
     assessment tool for bearing materials, where indications of the performance of the material can be
     known in hours, rather than days. We hypothesize that the results of nano-indentation and nano-wear
     testing are related directly to the results of AE testing.

     Abstract
     Self-lubricating polymeric materials are attractive candidates to be used as bearing materials in
     lightly loaded applications. In this study, miniature ball bearings made of steel, polytetrafluoroethylene
     (PTFE) reinforced with graphite, and polyether ether ketone (PEEK) are evaluated by means of nano-
     indentation and nano-wear tests. As quantified by the volume of the wear track, bearing steel has
     the best tribological performance, followed by the PEEK and PTFE. The volume of the wear track
     correlates with acoustic emissions measured during life testing. Other measurements available from
     a nano-wear test may indicate in-product performance; these include pile-up and the production of
     wear debris.

     Carlos Morillo, Ranjith-Kumar Sreenilayam-Raveendran, Michael H. Azarian and Michael Pecht
     CALCE (Center for Advanced Life Cycle Engineering) University of Maryland, College Park,
     MD 20742 USA
03 | Keysight | Evaluation of Bearing Materials Using NanoScale Wear Testing - Application Note



Experimental Procedure
Samples                                                                                  Wear Testing
Three different materials were selected for testing: bearing steel,                      The test method "G-Series Pass and Return Wear Test" used to
PTFE-graphite composite, and PEEK. These are the same samples                            perform one multi-pass, constant-load wear test on each sample.
used in a previous study [3]. Samples were cut and mounted in                            The chronology of a single test was as follows: The indenter profiled
epoxy, then ground and polished to a mirror-like finish.                                 the original surface along the length of the anticipated wear test,
                                                                                         then returned to its starting position (profile length = 120m,
Equipment                                                                                profile force = 50N). The indenter then performed a beginning
                                                                                         profile (10m, 50N), increased the applied force to the wear load
For all testing, the Keysight Technologies, Inc. G200 NanoIndenter                       and performed the first wear pass (100m, 20mN), then performed
was used, having an XP head with a Berkovich tip (20nm diameter),                        an ending profile (10m, 50N), and finally returned to its starting
and the continuous stiffness measurement (CSM) option.                                   position to complete the first wear cycle. The beginning and ending
                                                                                         profiles for each wear pass were used for leveling. Ten wear cycles
Indentation Testing                                                                      were performed in the same way (profile, wear, profile). After the
                                                                                         wear cycles, the indenter performed a final profile along the entire
The test method "G Series CSM Standard Hardness, Modulus and
                                                                                         length of the wear test (120m, 50N), then performed a final
Tip Cal method" was used for the indentation tests. As the indenter
                                                                                         cross-profile of the wear track (100m, 50N) at its midpoint.
was pressed into the material, a small oscillation (45Hz, 2nm) was
                                                                                         Each wear test returned measurements of scratch width, depth,
imposed in order to measure elastic modulus and hardness as a
                                                                                         deformation area, and pile-up. Post-test imaging of the wear
continuous function of penetration depth. Ten indentations were
                                                                                         tracks by scanning-electron microscope gave further qualitative
performed on each material to a peak depth of 1000nm. We used
                                                                                         information about each material. One wear test was performed on
data in the range of 900



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